Integrated ultra clean high-temperature and high-pressure vacuum sintering system

Release time: 2025-11-05 17:14:51  Number of views: 11

This system is a fully automatic, multi environment, integrated heat treatment equipment tailored for high-end material research and preparation. It innovatively integrates a high sealing glove box with a high-performance high-temperature and high-pressure vacuum well furnace, creating a complete, ultra clean and inert atmosphere protection platform that can transfer samples. This system completely solves the problem of exposing materials that are extremely sensitive to oxygen and moisture (such as lithium battery materials, metal powders, special alloys, superconducting materials, etc.) to the atmosphere during sintering, annealing, and synthesis processes, ensuring that the entire process of material pretreatment, loading, reaction, and removal is carried out in an extremely pure environment. It is the ultimate solution to improve the intrinsic properties of materials, obtain cutting-edge scientific research results, and prepare high-purity products

  

Product Details

Equipment Features:
1. Fully enclosed ultra clean system:
·The glove box is connected to the furnace body through a dedicated transition chamber to achieve non oxidative transfer of samples.
·The atmosphere inside the glove box (such as high-purity argon gas) can maintain a water oxygen value of<0.1ppm, providing the highest level of protection for the sample.
·Avoiding the pollution and oxidation risks caused by sample transfer in traditional equipment.
2. Extreme working condition handling capability:
·High vacuum: The maximum vacuum degree of the furnace chamber can reach the level of 10 ⁻⁵ Pa, effectively removing gas impurities in the system and preventing material oxidation at high temperatures.
·High temperature: Using high-quality alloy resistance wire heating, the maximum working temperature can reach 1100 ℃ -1200 ℃ (depending on the configuration), meeting the sintering temperature requirements of the vast majority of high-end materials.
·High pressure: Integrated with advanced gas pressurization system, it can achieve a uniform pressure environment of tens or even hundreds of bars in an inert atmosphere, used for hot pressing sintering, effectively improving material density.
3. Intelligent automation enhancement system:
·The furnace cover adopts an electric automatic lifting mechanism, which runs smoothly and has precise positioning.
·Linked with the control system, it can achieve one click opening/closing of the lid, greatly improving the safety and convenience of operation, while ensuring high repeatability of the process.
4. Precision process control:
·Equipped with a multifunctional touch screen human-machine interface and a built-in advanced programmable controller.
·Users can freely set and store complex temperature, pressure, and vacuum curves, realizing complex processes such as multi-stage temperature rise and fall, constant temperature and pressure, and automatic inflation.
·The system has complete data recording and fault diagnosis functions, ensuring the traceability of the process and the safe and reliable operation of the equipment.

Device Name

Integrated ultra clean high-temperature and high-pressure vacuum sintering system

Specification Model

NBD-HDDR-PT-T80

power supply

AC380V

rated power

5.2KW

Number of temperature zones

Single temperature and single control

temperature control accuracy

±1℃

sensor type

K-type thermocouple with a diameter of 2 * 350mm

Tmax

Vacuum state: 1100 ℃
High pressure state: 800 ℃ (2MPa)

Recommended heating rate

≤10℃/min

Temperature zone size and length

φ150*300mm

Reactor material and size

GH747 alloy
Size: 120*430mm, wall thickness 10mm (cavity size: 100*400mm)

Maximum travel of lifting mechanism

530mm

Dimensions inside the crucible

Φ26*52mm

Test electrode size

1.5-2mm

Torque wrench required for sealing the upper cover

60N∙m

furnace body dimensions

Glove box and furnace assembly: length 3550 * height 2110 * depth 1100mm
Electric control cabinet: length 680 * height 880 * depth 950mm
High vacuum unit: length 885mm * height 770 * depth 790mm

control system

1. Sintering process curve setting: dynamically display the set curve, and the equipment sintering can pre store multiple process curves, each of which can be freely set;
2. Pre order sintering is available to achieve unmanned sintering process curve sintering;
3. Real time display of sintering power, voltage and other information, recording of sintering data, and the ability to export for paperless recording;
4. Capable of remote control and real-time observation of equipment status;
5. Temperature correction: The difference between the main control temperature and the sample temperature is nonlinearly corrected throughout the sintering process.

heating element

Alloy resistance wire

temperature accuracy

±1℃

Net weight

750KG

Equipment usage precautions

Untrained personnel are not allowed to use glove boxes without authorization;
2. Prohibit the use of substances that can poison regenerated catalysts, such as thiol compounds;
3. Without permission, volatile solvents that may damage resin glass, such as acetone, shall not be used;
4. Contact the person in charge to remove the water probe before using volatile solvents;
5. When using volatile solvents, it is necessary to turn on the activated carbon circulation system;
When using the glove box, there should be no long nails and sharp objects (such as watches, jewelry, etc.) should not be worn;

Service Support

One year limited warranty, providing lifetime support (the warranty does not include consumable parts such as processing tubes and O-rings, please order replacement parts at the relevant product below)

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                     0371-6320 2805
After-sales service: 0371-6320 2805
MR. CAI: 181-0371-5723
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Ms.Huang: 188-3829-0748
Email : nbd@nbdkj.com
Address:8# zhuyuan, Xinhua subdistrict, Xinzheng, Zhengzhou, China
Contact Us
Sale Service: 0371-6320 2801
                      0371-6320 2805
After-sales service: 0371-6320 2805
MR. CAI: 181-0371-5723
Email : nbd@nbdkj.com
Address:8# zhuyuan, Xinhua subdistrict, Xinzheng, Zhengzhou, China
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