Equipment Features:
1. Closed loop ultra clean environment guarantee:
·Glove box active protection: provides an initial and reliable ultra-low water oxygen environment (H ₂ O&O ₂<0.1 ppm) for safe pre-treatment and furnace loading of samples.
·Seamless sample transfer: Through a dedicated transition chamber, the sample can be transferred between the glove box and the furnace without contamination, completely isolating the atmosphere.
2. Precise application of extreme working conditions:
·Vacuum and atmosphere protection: The furnace body has the ability to extract vacuum and can introduce high-purity inert gas. Through the classic logic of "first evacuate, then fill the atmosphere", the oxygen free environment inside the furnace is double guaranteed.
·Automatic lifting and precision temperature control: The electric automatic lifting furnace cover is linked with a programmable logic controller (PLC) to ensure precise and repetitive operation. Cooperate with multi-stage programmable temperature control to achieve complex sintering processes.
3. Intelligent integrated control:
·The unified control interface integrates all operations and data of the glove box, furnace body, vacuum system, gas path, and oxygen analyzer.
·Users can preset the "one click start" process formula, and the system automatically completes the entire process from vacuuming, gas washing, heating, insulation, monitoring to cooling, minimizing human intervention and errors.

Device Name

Fully automatic ultra clean vacuum sintering and quality monitoring system (Hastelloy oxygen free well furnace)

Specification Model

NBD-PG1200-20TI5LN

power supply

AC380V 50HZ

rated power

13KW

sensor type

K-type thermocouple Φ 2*350mm

Tmax

1200℃

Long term working temperature

1150℃

Recommended heating rate

≤10℃/min

Number of temperature zones

Single temperature and single control

Size of furnace temperature zone

Φ350*420mm

Reactor material and size

Hastelloy C276
A 2.3L corundum crucible (Φ 165 * 153mm) can be placed in a diameter of 273 * 585mm

One way float flowmeter

0.3-3L/min

Exhaust method

Electric ball valve KF25 interface, vacuum port KF25

Maximum stroke of lifting device

650mm

furnace body dimensions

Glove box and furnace section: length 3500 * height 1985 * depth 910mm
Glove box electrical control cabinet: length 850 * height 850 * depth 1350mm

control system

1. Sintering process curve setting: dynamically display the set curve, and the equipment sintering can pre store multiple process curves, each of which can be freely set;
2. Pre order sintering is available to achieve unmanned sintering process curve sintering;
3. Real time display of sintering power, voltage and other information, recording of sintering data, and the ability to export for paperless recording;
4. Capable of remote control and real-time observation of equipment status;
5. Temperature correction: The difference between the main control temperature and the sample temperature is nonlinearly corrected throughout the sintering process.

Hastelloy reaction chamber

heating element

Alloy resistance wire

temperature accuracy

±1℃

Net weight

About 950KG

Equipment usage precautions

Untrained personnel are not allowed to use glove boxes without authorization;
2. Prohibit the use of substances that can poison regenerated catalysts, such as thiol compounds;
3. Without permission, volatile solvents that may damage resin glass, such as acetone, shall not be used;
4. Contact the person in charge to remove the water probe before using volatile solvents;
5. When using volatile solvents, it is necessary to turn on the activated carbon circulation system;
When using the glove box, there should be no long nails and sharp objects (such as watches, jewelry, etc.) should not be worn;

Service Support

One year limited warranty, providing lifetime support (the warranty does not include consumable parts such as processing tubes and O-rings, please order replacement parts at the relevant product below)